3-Hydroxyacetophenone CAS NO.121-71-1

Superiority PackingStandard packaging includes the following: 25kg/drum Other package sizes are available upon request. StorageStore in a well-ventilated, cool, dry area, out of direct sunlight. Keep containers tightly closed when not in use. Period of validity24 months ? Product Superiority ? 1.High quality

Description:

Superiority

PackingStandard packaging includes the following: 25kg/drum Other package sizes are available upon request.

StorageStore in a well-ventilated, cool, dry area, out of direct sunlight. Keep containers tightly closed when not in use.

Period of validity24 months

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Product Superiority

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1.High quality with best price

2.Well reputation

3.Factory with strong supply ability

4. Prompt shipment

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Packing & Delivery

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FAQ

1. who are we? We are based in Shandong, China, start from 2014,sell to Southern Europe(00.00%),Domestic Market(00.00%),South America(00.00%),North America(00.00%),Eastern Europe(00.00%),Africa(00.00%),Eastern Asia(00.00%). There are total about 11-50 people in our office. 2. how can we guarantee quality? Always a pre-production sample before mass production; Always final Inspection before shipment3. why should you buy from us not from other suppliers? Have a strong ability to warehousing logistics and release permit of dangerous goods export right and use right, has a strong factory as a backstop. 4. what services can we provide? Accepted Delivery Terms: FOB,CFR,CIF,EXW; Accepted Payment Currency :USD; Accepted Payment Type: T/T,L/C; Language Spoken:English,Chinese

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Our services

<1> Free samples for customer further evaluation before order and after production.

<2>Quality controlling throughout the production,inspection and shipment.

<3> Packing according to customers requirements.

<4> the nearest port to customer site,very convenient for discharge

<5> Complete documents for customer customs clerance

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Details

Chemical Properties: Needle-like crystals. Melting point 95-97℃, boiling point 296℃, 153℃ (0.67kPa), relative density 1.099 (109℃), refractive index 1.5348. Soluble in ethanol, ether, chloroform, and benzene; slightly soluble in water; insoluble in petroleum ether.

Uses: 3-Hydroxyacetophenone can be used in organic synthesis and is an intermediate in the drug phenylephrine.

Production Method: Obtained by reacting m-aminoacetophenone with sodium nitrite. Water and concentrated sulfuric acid are added to a reaction vessel, and m-aminoacetophenone is added while stirring. Then, an aqueous solution of sodium nitrite is added dropwise while cooling, maintaining the temperature at 8-10℃. After the addition is complete, the temperature is slowly raised to above 90℃, and the reaction is continued with stirring for 1 hour. The solid precipitates upon cooling, is filtered, and the crude product is recrystallized from hot water to obtain m-hydroxyacetophenone. Yield: 65%.